Intergranular corrosion igc testing is the only corrosion test performed as a standardized predelivery test. Jan 29, 2021 astm a test, intergranular corrosion, igc, astm a practice, copper copper sulfate 16% sulfuric acid, astm a practice e strauss test. The results of the test is only a measure of intergranular corrosion. Sep 03, 2019 choosing an intergranular corrosion test method since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion igc much more rapidly than properly treated materials. Part of the advances in corrosion science and technology book series. Electrochemical qualification of biomedical implantable devices. Aug 15, 2019 strauss test specimens are boiled in a copper sulfate sulfuric acid mixture for 15 hours. Since high temperature processing such as heat treatment is a common practice, many. Astm a test, intergranular corrosion, igc, astm a practice, testing, india download as pdf file. Figure also shows specimen for astm a 262 practice e test. Inter granular corrosion can be detected by ultrasonic and eddy current methods. Intergranular corrosion is a localized attack along the grain boundaries, or immediately adjacent to grain boundaries, while the bulk of the grains remain largely unaffected.
It is often caused by improper processing of the metal during manufacture or improper heat. Sigma phase in wrought chromiumnickel molybdenum steels, which may or may not be visible in the microstructure, can result in high corrosion rates only. To minimize the costs and delivery time delays associated with purchasing type 304l stainless steel materials for service in nitricacidcontaining media, an alternative to the current oak ridge y12 plant requirement of testing in accordance with american society for testing and materials astm a 262, practice c the boiling nitric acid test, is being sought. From macroscopic imaging to scanning electron microscopy, element provides turnkey metallographic services using stateoftheart equipment.
Intergranular corrosion susceptibility of alloy 600 after autogenous. Astm a262 intergranular corrosion test igc intergranular corrosion is sometimes also called intercrystalline corrosion or interdendritic corrosion. Pdf assessment of intergranular corrosion in aisi type 316l. Evaluating chemical plant intergranular corrosion with metallography and xps chemical analysis. Sensitization refers to the precipitation of carbides at grain boundaries in a stainless steel or alloy, causing the steel or alloy to be. Intergranular corrosion igc is a form of localized corrosion characterized by preferential corrosion at grain boundaries or areas adjacent to them, with little or negligible attack on the grains. Intergranular corrosion and intergranular stress corrosion.
The first and fastest step is the astm a262 practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular corrosion. The test is generally performed for acceptance of materials, but not sufficient for rejection of. The moneypennystrauss test is also known as the strauss test, and has classifications including sis 117105, din 50914 and astm a262 practice e. G15 terminology relating to corrosion and corrosion testing. G67 test method for determining the susceptibility to intergranular corrosion of 5xxx series aluminum alloys by mass loss after exposure to nitric acid. The use of astm a262 practice a and e tests indicated sensitisation in base metal. The time and temperature required to produce susceptibility to intergranular attack iga is dependent on alloy composition, particularly the carbon content. We also offer nadcap accredited services for evaluating intergranular corrosion attack and oxidation igaigo. Intergranular corrosion behavior of nickel base superalloys 600, 690 and 693. Astm a is a screening test to help find batches that are incorrectly processed. The microstructure of metals and alloys is made up of grains, separated by grain boundaries.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Intergranular stress corrosion cracking of welded steel twi. The results of this test correlate reasonably well with those of astm g 28 and astm a 262 tests. Intergranular corrosion is localized attack along the grain boundaries, or immediately adjacent to grain boundaries, while the bulk of the grains remain largely unaffected. Speed of corrosion loss of mass in a fixed exposure time. Assessment of intergranular corrosion in aisi type 316l stainless. A novel preweld laser surface treatment for enhanced. Practice a, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to. Astm international astm a26298 standard practices for. Jan 30, 2021 astm a is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
An electrochemical reactivation epr test is used to study the effect of sensitization on intergranular corrosion and intergranular stress corrosion cracking behavior. Classification of the structure after a262 practice a analysis will determine if the material is acceptable or if additional testing is required. They are carried out as a rule on samples from finished tubes in the asdelivered condition or on material that has been sensitized, i. Astm a262 is the most common test for sensitization, and there are five common versions within the method that are used. Intergranular corrosion induced by environmental stresses is termed stress corrosion cracking.
Intergranular corrosion can be prevented by altering the environment as shown in table iii. Small amounts of iron in aluminum, wherein solubility of iron is low, have been shown to segregate in the grain. We offer professional photography to document performance changes. Influence of rolling and annealing parameters on the intergranular corrosion was studied by astm g67 standard test nitric acid mass loss namlt, using optical microscopy om, scanning electron microscopy sem and energydispersive xray spectroscopy. A wellknown example of igc is the sensitisation of austenitic 18cr8ni stainless steels. There are a number of recognised tests when it comes to the intergranular corrosion testing of corrosion resistant alloys cra.
How to study intergranular corrosion igc of nickel and. Most alloys are susceptible to intergranular corrosion, also known as intergranular attack iga, when exposed to specific environments. Intergranular corrosion igc is an effective test to screen the corrosion resistance of materials under certain conditions. Corrosion testing techniques and evaluation practices used. G1 practice for preparing, cleaning, and evaluating corrosion test specimens. Electrochemical etching was made in oxalic acid solutions as described in the astm a262 practice. Intergranular corrosion an overview sciencedirect topics. In such cases, the acid corrosion test is applicable, but not the oxalic acid etch test. Sensitization and intergranular corrosion of stainless. Standard practices for detecting susceptibility to. Similarly to other forms of localized corrosion, it mainly occurs on passive alloys exposed to specific corrodents. Ferritic,austenitic, and ferriticaustenitic duplex stainless steels corrosion test in media containing sulfuric acid 3. Astma262 standard practices for detecting susceptibility.
Intergranular corrosion igc, also known as intergranular attack iga, is a form of corrosion where the boundaries of crystallites of the material are more. In the presence of tensile stress, cracking may occur along grain boundaries and this type of corrosion is frequently called interranular stress corrosion cracking igscc or simply. What is astm a262 intergranular corrosion test igc china. Astm a262 practice a is an oxalic acid is the rapid 4 hour screening method, often used as a first pass to determine the susceptibility to intergranular corrosion.
Intergranular corrosion behavior of nickel base superalloys 600. Intergranular corrosion igc test astm a262 igc practice c test in progress igc situation can happen in otherwise corrosion resistant alloys, when the grain boundaries are depleted, known as grain boundary depletion, of the corrosion inhibiting elements such as chromium by some mechanism. Removing copper sulfate from normal h2so4 at 900c test 18 prevents intergranular corrosion test 16. Mar 19, 2020 intergranular corrosion test igc per astm a at tcr engineering services, several methods exist for the testing of intergranular corrosion. Astm a262 15 standard practices for detecting susceptibility to. This form of corrosion is usually associated with chemical segregation effects impurities have a tendency to be enriched at grain boundaries or specific phases.
Susceptibility to intergranular attack associated with the precipitation of chromium carbides is readily detected in all five tests. Jun 14, 2020 these practices include five intergranular corrosion tests, astj practice e, the strauss test, is performed to assess attack associated with chromiumrich carbide formation. The first and fastest step a62 the astm a practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular corrosion. Intergranular corrosion is also known as inter granular attack iga.
The test methods outlined in astm a262 have been developed to detect susceptibility to intergranular attack in austenitic stainless steels. Corrosion testing techniques and evaluation practices used in. G 67 93 test method for determining the susceptibility to intergranular corrosion of 5xxx series aluminum alloys by mass loss after exposure to nitric acid namlt test g 69 97 practice for measurement of corrosion potentials of aluminum alloys. Assessment of electrochemical potentiokinetic reactivation. The purpose of this study is to put forward knowledge about the. Astm a is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. Schedule 80 stainless pipe, with intergranular stress corrosion igscc and fatigue cracks, as well as 844.
Our failure analysis lab is equipped with innovative technology utilizing analytical and component testing to gather valuable insight into the causes of. Corrosion resistance of injectionmolded 174ph steel in. Oct 04, 2019 practice a, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. This part of iso 3651 specifies methods for the determination of the resistance to intergranular corrosion of ferritic, austenitic and ferriticaustenitic duplex stainless steels in media containing sulfuric acid. Each has similarities and differences both in the test solution, the test sample and the passfail criteria, and it is a good idea to familiarise yourself with these. Intergranular corrosion igc is strongly associated with the properties and microstructure of a metal. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is wstm as effective for intergranular attack caused by other means. Note 1for each corrosion test, the types of susceptibility to intergranular attack detected are given along with the grades of stainless steels in which they may be found. Feb 06, 2011 intergranular corrosion igc microstructure of metals and alloys is made up of grains separa ted by grain boundaries intergranular corrosion is a localized attack along the grain bo undaries, or immediately adjacent to grain boundaries, while the bulk of t he grains remain largely unaffected igc is associated.
It also specifies the purposes which may be assigned to the test. Jun 16, 2020 practice a, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. Astm a262, practice a, b, c, and f intergranular corrosion. Intergranular corrosion sensitization testing per astm a. In this study, the degree of sensitization was examined in aisi. This form of corrosion is usually associated with chemical segregation effects impurities have a tendency to be enriched at grain boundaries or specific phases precipitated on the grain boundaries. Practice for conducting acidified copper sulfate test for intergranular attack in. These lists may contain grades of steels in addition to those given in the rectangles. Astm a262 practice a, b, c, e and f testing g2mt laboratories.
When an alloy is undergoing this type of corrosion, its rate of weight loss will. Vaevaluating intergranular corrosion asm international. D1193 specification for reagent water e3 guide for preparation of metallographic specimens e407 practice for microetching metals and alloys g1 practice for preparing, cleaning, and evaluating corrosion test specimens. Test of resistance to intergranular corrosion of stainless. The possibility of using eddy current testing ect to detect sensitisation and igc was also assessed. G 2802 standard test methods of detecting susceptibility to intergranular corrosion in wrought. Intergranular corrosion tests applied technical services. Intergranular corrosion, dlepr test method, austenitic stainless steel. Intergranular corrosion facts and how to reduce the risk.
Note 1for each corrosion test, the types of susceptibility to intergranular attack detected are given along with the grades of. Intergranular corrosion testing of austenitic stainless. In smithells metals reference book eighth edition, 2004. Sensitization of 304 stainless steel using the astm g108 test method.
Intergranular attack astm a coloradometallurgicalservices. Astm a262 intergranular corrosion testing and analysis. Webcorr provides corrosion consultancy services, corrosion expert witness and corrosion short courses for inhouse training, online and distance learning. A summary of the results of the phase ii igscc tests is presented in table 3b and 3c. Intergranular corrosion forms along the grain structure of metal. Nov 05, 20 the moneypennystrauss test heat treats the sample in the sensitizing temperature range in order to determine the materials resistance to intergranular corrosion. Determine corrosion rates for metal in an aqueous environment. Aug 17, 2020 astm a test, intergranular corrosion, igc, astm a practice, testing, india download as pdf file. The standards and methods for intergranular corrosion test. Intergranular corrosion testing of austenitic stainless steels in nitric. It describes the most serious forms of structuredependent corrosion, such as stress corrosion cracking and exfoliation, in aluminum alloys including strainhardened 5xxx almg alloys and heat. Astm a intergranular corrosion testing and analysis. Our experts at ats are adept in investigating the corrosion of alloys and metals.
The oxalic acid etch test is rapid and nondestructive, but not quantitative. Iso 36512 determination of resistance to intergranular corrosion of stainless steelspart 2. Mar 28, 2016 intergranular corrosion of an alloy may be caused by impurities at the grain boundaries enrichment of one of the alloying elements depletion of one of the elements that affects its corrosion resistance in grain boundary areas. Detecting susceptibility to intergranular attack in austenitic stainless. Mar 02, 2020 the test is generally performed for acceptance of materials, but not sufficient for rejection of materials. G 11092 standard practice for evaluating intergranular corrosion resistance. This practice describes the procedure by which the coppercopper sulfate% sulfuric acid test is conducted to determine. Intergranular corrosion igc microstructure of metals and alloys is made up of grains separa ted by grain boundaries intergranular corrosion is a localized attack along the grain bo undaries, or immediately adjacent to grain boundaries, while the bulk of t he grains remain largely unaffected igc is associated. In some circumstances, grain interfaces are extremely reactive, leading to corrosion.
Sep 18, 2019 astm a test, intergranular corrosion, igc, astm a practice, testing, india download as pdf file. This part of iso 3651 specifies methods for the determination of the resistance to intergranular corrosion of ferritic,austenitic and ferriticaustenitic duplex stainless steels in media containing sulfuric acid. They range from metallographic analysis of the microstructure to immersion corrosion tests in various chemical solutions. Practice b, also known as the streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. Jul 04, 2019 choosing an intergranular corrosion test method since high temperature processing such prctice heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. Astm a is the specification which governs five practices used to determine if the. Detecting susceptibility to intergranular attack in austenitic stainless steels. These specimens will have low corrosion rates in certain corrosion tests and therefore can be eliminated screened from testing as acceptable. Graphitic corrosion in grey cast iron investigation. Intergranular corrosion testing of austenitic stainless steels in nitric acid solutions g o h whillock and b f dunnett bnfl, b170, sellafield, seascale, cumbria ca20 1pg u. Apart from a 262 practice a test, all the other tests are destructive in nature. Passfail 3 different types of stainless steels, showing various resistances to intergranular corrosion.
Immersion corrosion metallurgical engineering services. Intergranular corrosion in metals 4 causes of this. Strauss, huey and streicher are the common test methods. Intergranular corrosion of ironnickelchromium alloys springerlink. All different forms of corrosion are explained by nace certified corrosion specialist.
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